Search results for "Amnesic shellfish poisoning"

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Development of a pressurised liquid extraction and liquid chromatography with electrospray ionization-tandem mass spectrometry method for the determi…

2006

Amnesic shellfish poisoning (ASP) is a potentially lethal human toxic syndrome which is caused by domoic acid (DA) that originates in marine phytoplankton belonging to the Pseudonitzschia genus. A confirmatory and sensitive procedure has been developed and validated for the determination of DA in shellfish. The proposed method includes pressurised liquid extraction (PLE) with methanol/acetone (9:1), florisil ® cleanup purification inside the PLE extraction cell and detection by liquid chromatography (LC) coupled to electrospray ionization in positive mode tandem mass spectrometry (ESI-MS–MS). Comparison of ionization sources (ESI, atmospheric pressure ionization (APCI) atmospheric pressure …

Detection limitElectrospraySpectrometry Mass Electrospray IonizationChromatographyKainic AcidElectrospray ionizationOrganic ChemistryAnalytical chemistryDomoic acidAtmospheric-pressure chemical ionizationGeneral MedicineTandem mass spectrometryBiochemistryHigh-performance liquid chromatographySensitivity and SpecificityAnalytical Chemistrychemistry.chemical_compoundchemistryTandem Mass SpectrometryAmnesic shellfish poisoningAnimalsChromatography LiquidShellfishJournal of chromatography. A

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